Bis(N-ethyl-N-methyldithiocarbamato-κ2S,S′)diphenyltin(IV)
نویسندگان
چکیده
منابع مشابه
N-Ethyl-N-phenyl-N′-tosylformamidine
The title compound, C(16)H(18)N(2)O(2)S, was obtained as an unexpected product while attempting to form carbon-nitro-gen bonds by catalytic amidation. The mol-ecule displays an E conformation about the C=N double bond. The planes of the two aromatic rings in the mol-ecule form a dihedral angle of 47.06 (9)°.
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In the title mol-ecule, C(9)H(9)N(3)O(5), the dihedral angle between the mean planes of the amide group and the benzene ring is 31.24 (14)°. In the crystal, N-H⋯O hydrogen bonds link the mol-ecules to form one-dimensional chains propagating in [100].
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The title compound, [Sn(C(6)H(5))(3)(C(9)H(10)NS(2))], has two independent mol-ecules in the asymmetric unit and each features a tetra-hedrally coordinated Sn(IV) atom as the dithio-carbamate ligand coordinates in a monodentate fashion. As the non-coordinating thione S atom is proximate to the Sn atom [Sn⋯S(thione) = 3.1477 (6) and 2.9970 (5) Å for the independent mol-ecules], distortions from ...
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ژورنال
عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online
سال: 2010
ISSN: 1600-5368
DOI: 10.1107/s1600536810007427